GINAPS

In vitro studies and preliminary in vivo evaluation of silicified concentrated collagen hydrogels

Hybrid and nanocomposite silica-collagen materials derived from concentrated collagen hydrogels were evaluated in vitro and in vivo to establish their potentialities for biological dressings. Silicification significantly improved the mechanical and …

Methods for prevention, diagnosis and treatment achieved with the aid of sol-gel chemistry

The solgel process has several well-known advantages such as high purity precursors, homogeneity of the obtained material and especially the possibility of making hybrids and composite materials with new chemical and mechanical properties. This …

Removal of dyes from water using chitosan hydrogel/SiO2 and chitin hydrogel/SiO2 hybrid materials obtained by the sol-gel method

This work describes the synthesis of chitosan hydrogel/SiO2 and chitin hydrogel/SiO2 hybrid mesoporous materials obtained by the sol-gel method for their use as biosorbents. Their adsorption capabilities against four dyes (Remazol Black B, …

Synthesis and characterisation of a silicon oxide film solid-phase extraction system for lead traces determination: An all the way green analytical method

In this work, an all the way green analytical procedure based on a silicon oxide film-solid phase extraction system is proposed for lead traces determination. From the synthesis of a solid phase extraction (SPE) system and throughout the metal …

XPS studies on the Cu(I,II)-polyampholyte heterogeneous catalyst: An insight into its structure and mechanism

A complex between Cu(II) and a polyampholyte synthesized from methacrylic acid, imidazole and ethyleneglycol diglycidyl ether was used as a heterogeneous catalyst for hydrogen peroxide activation and degradation of chlorophenols. The material was …

Egg white lysozyme purification with a chitin-silica-based affinity chromatographic matrix

A composite biosorbent retaining non-covalently bound chitin in between layers of a silicon oxide matrix was assessed for lysozyme purification from undiluted egg white. The matrix can be shaped with big size and high density, thus allowing its …

NMR characterization of hydrate and aldehyde forms of imidazole-2- carboxaldehyde and derivatives

The existence and stability of the aldehyde-hydrate form of imidazole-2-carboxaldehyde (4) were studied using FTIR together with solution- and solid-state NMR experiments. The results allowed us to conclude that the hydrate form was stable and …

Effect of various parameters on viability and growth of bacteria immobilized in sol-gel-derived silica matrices

Immobilized bacteria are being extensively used for metabolite production, biocatalysts, and biosensor construction. However, long-term viability and metabolic activity of entrapped bacteria is affected by several conditions such as their …

Development and characterization of a new polyampholyte-surfactant complex applied to the solid phase extraction of bisphenol-A

This paper presents a material that has both hydrophilic and hydrophobic domains, obtained by combination of a polyampholyte with a surfactant. This material was fully characterized by different spectroscopic techniques and microscopy. Bisphenol-A …

Antibody detection employing sol-gel immobilized parasites

Immunofluorescence assay (IFA) and immunoperoxidase assay (IPA) are useful diagnostic techniques for specific antibody detection for different diseases. Both involve several alternatives for immobilization of cells, such as solvent or heat fixation. …